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Beilstein J. Org. Chem. 2016, 12, 2668–2672, doi:10.3762/bjoc.12.263
Graphical Abstract
Scheme 1: Structures of the boronic acid compounds used in this study (i.e., SPB and pVPB/NaSS).
Figure 1: Time–conversion plots for the formose reaction using 200 mM formaldehyde, 20 mM calcium hydroxide, ...
Figure 2: HPLC charts for standard samples (a) and products of the formose reaction in the absence (b) and pr...
Figure 3: 1H (a, b, and c) and 13C NMR spectra (d, e, and f) for the products of the formose reaction in the ...
Figure 4: ESIMS data for the products of the formose reaction in the presence of 10 mM SPB (a) and 20 g L−1 p...
Beilstein J. Org. Chem. 2016, 12, 2663–2667, doi:10.3762/bjoc.12.262
Scheme 1: Structures of AOT, TX, and CTAB.
Figure 1: Time–conversion plots for formose reactions in an aqueous solution (black) and in water pools of AO...
Figure 2: Time–conversion plots for formose reactions in AOT reverse micelles of different w at 30 (a), 45 (b...
Figure 3: Convmax and k2 as function of w for formose reactions in water pools of AOT reverse micelles at 30 ...
Figure 4: 13C NMR spectra for the products of the formose reaction carried out in AOT reverse micelles of w =...